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Description of Individual Course Units| Course Unit Code | Course Unit Title | Type of Course Unit | Year of Study | Semester | Number of ECTS Credits | | FBK635-13 | LABORATORY TECHNIGUES | Compulsory | 1 | 2 | 6 |
| | Level of Course Unit | | Second Cycle | | Objectives of the Course | | to teach to work in the labratory, safely.
to teach monitoring of the synthesis reaction and how to do separation and purification after the reaction | | Name of Lecturer(s) | | Lecturers of Chemistry Department | | Learning Outcomes | | 1 | to know safe working and first aid in the lab | | 2 | to know glassware and set up necessery reaction aparatus | | 3 | to monitor the progress of the reaction in the synthesis reaction | | 4 | to use methods of separation and purification of compounds in the reaction mixture | | 5 | to have knowledge about different reactions and reaction mediums |
| | Mode of Delivery | | Formal Education | | Prerequisites and co-requisities | | None | | Recommended Optional Programme Components | | None | | Course Contents | | Laboratory Safety
Keeping of Experimental Results and Yield Calculation
Glassware
General Laboratory Operations
Drying and Purification procedures
Working with gases
Working under inert Atmosphere
Implementation of the reaction, various reaction Mechanisms
Termination of the reaction and Separation of the crude product, The different reaction media
Purification and Separation Processes
Special Reactions
| | Weekly Detailed Course Contents | |
| 1 | Safety in Laboratory, Reducing the Risks and Firstaid | | | | 2 | Maintaining Records and Calculation of Yield | | | | 3 | Glassware, Sintered Glassware, Cleaning the Glassware | | | | 4 | General Laboratory Procedures, Mixing, Heating, Cooling, Filtration and Drying | | | | 5 | Preparing Reactives and Solvents for Reactions, Drying and Purification of Some Solvents, Purification of Some Solid Reactives | | | | 6 | Working with Gases, Pressured Gas Cyclinder, Gas Traps, Preparing of Some Gases in Laboratory | | | | 7 | Working in Inert Atmosphere, Weighing Reactive Solids, Transfering Liquids to the Reaction System, Setting the Reaction Systems | | | | 8 | Midterm | | | | 9 | Execution of Reactions, Various Reaction Systems, Changing the Chemical Equilibrum in Reactions; Removing one of Products, Removing Water | | | | 10 | Ending the Reaction and Separating the Crude Product
General Ending Procedures; Strong Basic Dry Medium Reactions, Neutral Dry Medium Reactions, Strong Acidic Dry Medium Reactions, Acidic or Basic Watery Reactions
| | | | 11 | Genel Ayırma İşlemleri; Tek Fazlı Katı Sistemler, Tek Fazlı Sıvı Sistemler, Katı-Sıvı İki Fazlı Sistemler, Sıvı-Sıvı İki Fazlı Sistemler | | | | 12 | Purificatin Processes, Crystallization, Distillation; Simple, Steam, Fractional Distillations and Distillation under Vacuo, Sublimation, Extraction;Liquid-Liquid Extraction, Solid-Liquid Extraction | | | | 13 | Chromatography; Column Chromatography, Thin Layer Chromatography, Preparative Chromatography | | | | 14 | Special Reactions, Catalytic Hydrogenation, High Pressure Reactions, Ozonizing Reactions, Gas Phase Reactions, | | | | 15 | Photochemical Reactions, Electrochemical Reactions, Liquid Ammonia Reactions | | | | 16 | Final Exam | | |
| | Recommended or Required Reading | | Organik Laboratuvar Teknikleri, N. Öcal, F. Aydoğan, YTÜ Basım-Yayın Merkezi, İstanbul, 2004
Organik Kimya Laboratuvar Teknikleri, İ.E. Gümrükçüoğlu, M. Kepez, M. Odabaşoğlu,, OMÜ Basım-Yayın Merkezi, Samsun, 1996
| | Planned Learning Activities and Teaching Methods | | | Assessment Methods and Criteria | |
| SUM | 0 | |
| SUM | 0 | | Yarıyıl (Yıl) İçi Etkinlikleri | 40 | | Yarıyıl (Yıl) Sonu Etkinlikleri | 60 | | SUM | 100 |
| | Language of Instruction | | Turkish | | Work Placement(s) | | None |
| | Workload Calculation | |
| Midterm Examination | 1 | 2 | 2 | | Final Examination | 1 | 2 | 2 | | Quiz | 5 | 0.5 | 2.5 | | Attending Lectures | 14 | 3 | 42 | | Laboratory | 10 | 3 | 30 | | Report Preparation | 5 | 3 | 15 | | Seminar | 1 | 10 | 10 | | Individual Study for Mid term Examination | 8 | 7 | 56 | | Individual Study for Final Examination | 8 | 9 | 72 | |
| Contribution of Learning Outcomes to Programme Outcomes | | LO1 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | | LO2 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | | LO3 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | | LO4 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | | LO5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 |
| | * Contribution Level : 1 Very low 2 Low 3 Medium 4 High 5 Very High |
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